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24"L 3-Zone Tube Furnace w/ Optional Quartz Tube & Flange (60 - 130mm, 1200C Max.) -OTF1200XIIIS

24"L 3-Zone Tube Furnace w/ Optional Quartz Tube & Flange (60 - 130mm, 1200C Max.) -OTF1200XIIIS

SKU: otf-1200x-iii-s-ul

Price: RFQ

Specifications

Please view " Tailoring the Edge Structure of Molybdenum Disulfide towards Electrocatalytic Reduction of Carbon Dioxide " published by ACS Nano, Dec 07, 2016, in which an MTI OTF-1200X three-zone furnace was used for Ta and Nb-doped MoS2 synthesis. OTF-1200X-III-S is 24" Long ( 6"+12"+6") split-able three-zone tube furnace with quartz tube (size selectable) and conventional flange. Three 30 segments temperature controllers are installed with K-type thermal couples. Microprocessor-based self-tuning PID provides excellent control with no overshooting and +/- 1 °C accuracy. It is an excellent furnace for sample annealing, diffusion, and sintering in the various gas atmosphere up to 1200°C. SPECIFICATIONS: Furnace structure Double-layer steel case with two cooling fans which ensure low surface temperature; Energy-saving high purity fibrous alumina insulation; Two fibrous ceramic tube blocks are included for blocking heat radiation from inside of the tube. ( Ceramic blocks must be fully inserted into the furnace chamber before heating ). Quartz block ( Optional ) is ideal for more cleanness and a higher achievable vacuum. The furnace can be separated from the temperature controller and place it on remote location Click here to choose a crucible Multi-Stack Quartz Thermal Block fits for OTF1200XIIIS4 Rated voltage AC 208-240V Single Phase, 50/60 Hz (30A breaker required; Powder cord is included without plug) Power consumption 5KW Max. Heating elements Fe-Cr-Al Alloy doped by Mo Heating zone length Three zones: 610mm (24") in total Z1 - Z2 - Z3152.4mm (6") + 304.8mm (12") + 152.4mm (6") +/-1ºC Constant Temperature Zone: 260 mm length +/-2ºC Constant Temperature Zone: 480 mm length (click the pic below for detail) Fused Quartz Tube Model: OTF-1200X-III-S-UL-60 60 O.D x 55 I.D x 1200 L (mm) Model: OTF-1200X-III-S-UL-80 80 O.D x 72 I.D x 1200 L (mm) Model: OTF-1200X-III-S-UL-100 101 O.D x 92 I.D x 1200 L (mm) Model: OTF-1200X-III-S-UL-5 130 O.D x 122 I.D x 1200 L Warning: The tube furnaces with quartz tube are designed for use under vacuum and low pressure < 0.12 Mpa (absolute pressure) Heating temperature Max. Heating Temperature: 1200°C (<1 hour) Continuous Heating Temperature: 1100°C Max. Heating Rate: 20°C/min Temperature Controllers Three MTE certified Temperature controller with 30 programmable segments Built-in PID Auto-Tune function with overheating & broken thermocouple protection. Over-temperature protection and alarm allow for operation without an attendant. +/- 1 ºC temperature accuracy. Three K-type thermocouples (one for each zone). RS485 Communications Port. European Temperature Controllers (optional upgrade) 1 heating channel 1 program of 8 or 24-segment Alarm Relay: Form 'A' and Form ‘C’ built-in Digital Communications: RS485 Temperature Accuracy: ± 0.1ºC Recipes: Using a PC tool recipes can be created that can be used to change the operating parameters of the 3000 simply by selecting a new recipe via the HMI. This is very useful where multiple products are processed using the same controller but require different parameters to be set. Vacuum Flange and Gauge One pair of SS 304 vacuum flange with double high-temperature silicone O-ring is Included Default flange with 1/4'' Bard fittings, 1/4'' tube feedthrough port (for 1/4" O.D thermocouple insert) and a KF25 vacuum portclick bottom left picture to see details ) One Vacuum/ pressure gauge is installed on one side flange The vacuum level can reach 10E-2 torr by the quality mechanical vacuum pump and 10E-5 torr by a turbo pump Optional: You may choose a hinged type flange ( see pic below middle ) to make sample loading at easy. You may order the digital molecular pump for a faster and better vacuum You may order flange support to avoid tube rotating ( click Pic below right ) Laptop, software &l(Optional) Brand new laptop with Microsoft Windows 10 and Microsoft Office 2013 (30-day free trial) 9ncluded Labview Based Temperature Control System ( MTS01 ) enables users to edit temperature profiles, manage heat-treatment recipes, and record, and plot data for MTI furnaces. A wireless remote control provides up to 300 meters of operating range. Compliance CE certified NRTL or CSA certification is available upon request at the extra cost Application Notes Please click the picture below to learn how to create a temperature gradient ( pic.1) Order a temperature calibration kit by clicking picture 2. A ttention : A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure below 3PSI for safe operation. Click here to learn about the installation of a gas regulator. (pic.3) The automatic vacuum-sealed sliding device is available for fast heating and cooling ( Pic. 4) pic.1 pic.2 pic.3 Pic. 4 How to set up a quartz tube and vacuum flange. How to calibrate for an accurate temperature inside the tube furnace. STANDARD PACKAGE WITH FURNACE: No. NAME Qty PIC OTF-1200X-III-S-60 OTF-1200X-III-S-80 OTF-1200X-III-S-4 OTF-1200X-III-S-130 1 Fused quartz tube 1 pc QZTube-60GE-1200 QZTube-80D-48 QZTube-100 QZTube-125GE-1200 2 Alumina fiber foam tube block 2 pcs F-T-block-52 F-T-block-70 F-T-block-92 F-T-block-125 3 Hook for moving the sample 1 pc FLG-kit-2 FLG-kit-2 FLG-kit-2 FLG-kit-2 4 Metric Hex-wrenches 1 set √ √ √ √ 5 Vacuum flanges 1 pair FL-60 FL-80 FL-125 AVAILABLE OPTIONAL ACCESSORY: Part No. Description Quick Link MTS02 Computerized Temperature Control System High vacuum station (Mechanical pump + turbo molecular pump.) Gas mix station (Float flow meter / Mass flow meter) (2, 3, 4channels selectable) Compact Flow Meter (float flow meter/mass flow meter) QBlock-90 90mm O.D heat-insulating quartz block Quartz Boats /crucible /container /sample holder FM-Cart Heavy Duty Mobile Car for All MTI Tube and Box Furnaces

Furnace structure


  • Double-layer steel case with two cooling fans which ensure low surface temperature;
  • Energy-saving high purity fibrous alumina insulation;
  • Two fibrous ceramic tube blocks are included for blocking heat radiation from inside of the tube. (Ceramic blocks must be fully inserted into the furnace chamber before heating).
  • Quartz block (Optional) is ideal for more cleanness and a higher achievable vacuum.
The furnace can be separated from the temperature controller and place it on remote location
                   
Rated voltage AC 208-240V Single Phase, 50/60 Hz (30A breaker required; Powder cord is included without plug)
Power consumption 5KW Max.
Heating elements Fe-Cr-Al Alloy doped by Mo
Heating zone length
  • Three zones: 610mm (24") in total
  • Z1 - Z2 - Z3152.4mm (6") + 304.8mm (12") + 152.4mm (6")
  • +/-1ºC Constant Temperature Zone: 260 mm length
  • +/-2ºC Constant Temperature Zone: 480 mm length (click the pic below for detail)
Fused Quartz Tube
Quartz Tube: 216 OD x 208 IDx 1020L mm( 8.5"OD x 8.2" x 40"L) for DIY Tube Furnace - EQ-QZTube-216FE
Model: OTF-1200X-III-S-UL-60
60 O.D x 55 I.D x 1200 L (mm)
Model: OTF-1200X-III-S-UL-80
80 O.D x 72 I.D x 1200 L (mm)
Model: OTF-1200X-III-S-UL-100
101 O.D x 92 I.D x 1200 L (mm)
Model: OTF-1200X-III-S-UL-5
130 O.D x 122 I.D x 1200 L
Warning: The tube furnaces with quartz tube are designed for use under vacuum and low pressure < 0.12 Mpa (absolute pressure)
Heating temperature
  • Max. Heating Temperature: 1200°C (<1 hour)
  • Continuous Heating Temperature: 1100°C
  • Max. Heating Rate: 20°C/min
Temperature Controllers

  • Three MTE certified Temperature controller with 30 programmable segments
  • Built-in PID Auto-Tune function with overheating & broken thermocouple protection.
  • Over-temperature protection and alarm allow for operation without an attendant.
  • +/- 1 ºC temperature accuracy.
  • Three K-type thermocouples (one for each zone).
  • RS485 Communications Port.
European Temperature Controllers (optional upgrade)
  • 1 heating channel
  • 1 program of 8 or 24-segment
  • Alarm Relay: Form 'A' and Form ‘C’ built-in
  • Digital Communications: RS485
  • Temperature Accuracy: ± 0.1ºC
  • Recipes: Using a PC tool recipes can be created that can be used to change the operating parameters of the 3000 simply by selecting a new recipe via the HMI. This is very useful where multiple products are processed using the same controller but require different parameters to be set.
Vacuum Flange and Gauge
  • One pair of SS 304 vacuum flange with double high-temperature silicone O-ring is Included
  • Default flange with 1/4'' Bard fittings, 1/4'' tube feedthrough port (for 1/4" O.D thermocouple insert) and a KF25 vacuum portclick bottom left picture to see details )
  • One Vacuum/ pressure gauge is installed on one side flange
  • The vacuum level can reach 10E-2 torr by the quality mechanical vacuum pump and 10E-5 torr by a turbo pump
  • Optional:
    • You may choose a hinged type flange ( see pic below middle ) to make sample loading at easy.
    • You may order the digital molecular pump for a faster and better vacuum
    • You may order flange support to avoid tube rotating ( click Pic below right )
                 
Laptop, software &l(Optional)
  • Brand new laptop with Microsoft Windows 10 and Microsoft Office 2013 (30-day free trial) 9ncluded
  • Labview Based Temperature Control System (MTS01)enables users to edit temperature profiles, manage heat-treatment recipes, and record, and plot data for MTI furnaces.
  • A wireless remote control provides up to 300 meters of operating range.
Compliance
  • CE certified
  • NRTL or CSA certification is available upon request at the extra cost
Application Notes


pic.1 pic.2 pic.3Pic. 4
,
No. NAME Qty PIC OTF-1200X-III-S-60 OTF-1200X-III-S-80 OTF-1200X-III-S-4 OTF-1200X-III-S-130
1 Fused quartz tube 1 pc
QZTube-60GE-1200 QZTube-80D-48 QZTube-100

QZTube-125GE-1200

2 Alumina fiber foam tube block 2 pcs
F-T-block-52 F-T-block-70 F-T-block-92 F-T-block-125
3 Hook for moving the sample 1 pc
FLG-kit-2 FLG-kit-2 FLG-kit-2 FLG-kit-2
4 Metric Hex-wrenches 1 set
5 Vacuum flanges 1 pair

FL-60 FL-80 FL-125
,
Part No.
Description
Quick Link
MTS02 Computerized Temperature Control System

High vacuum station (Mechanical pump + turbo molecular pump.)

Gas mix station (Float flow meter / Mass flow meter) (2, 3, 4channels selectable)

Compact Flow Meter (float flow meter/mass flow meter)
QBlock-90 90mm O.D heat-insulating quartz block 

Quartz Boats /crucible /container /sample holder
FM-Cart
Heavy Duty Mobile Car for All MTI Tube and Box Furnaces

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