1200 °C Max 6" Automated Tube Furnace for AI Material Research - OTF1200XS6-ASD

1200 °C Max 6" Automated Tube Furnace for AI Material Research - OTF1200XS6-ASD

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1200 °C Max 6" Automated Tube Furnace for AI Material Research - OTF1200XS6-ASD

1200 °C Max 6" Automated Tube Furnace for AI Material Research - OTF1200XS6-ASD

SKU: otf-1200xs6-asd

Price: RFQ

Description

OTF-1200XS6-ASD is a 6" OD automated tube furnace up to 1100°C. It automates the pump-purge cycles, gas flow, vacuum, heating, and cooling in a sequence. The sliding flange simplifies sample loading and retrieval for conventional tube furnaces. With assistance of a robotic arm, it realizes continuous operation 24×7 to accelerate next-generation material discovery. It also supports remote PC control, monitoring, and data logging and links up to 8 furnaces.

Note: Please check out Prof. Ceder's Group using this furnace for an excellent article: An autonomous laboratory for the accelerated synthesis of novel materials 

SPECIFICATIONS:

Utility
  • 208-240VAC, 50/60Hz, 6 kW
  • Recirculating chilled water
Automation Process

  • Sample loading (assisted by a robotic arm)
  • Pump-purge cycles
  • Steady gas flow
  • Heating, dwelling, and cooling
  • Sample retrieval (assisted by a robotic arm)
Furnace 
  • Double-layer steel structure with cooling fans
  • High-purity alumina fibrous insulation for better energy saving
  • Motorized sliding sample stage for sample loading and retrieval. 
Working Temperature
  • <1100°C
Heating Area
  • 175+175 mm, dual heating zones
Temperature Uniformity
  • 120 mm @ ± 5°C
Heating Element
  • FeCrAl: Mo
Thermocouple
  • K type
Heating Rate
  • ≦10°C/min
Tube
Temperature Controller
  • PID programmable temperature controller
  • Up to 50 temperature segments. 
  • Control accuracy ±1°C
Flange Set
  • 304 stainless steel water-cooled flanges
  • Ø12 push-to-connect chilled water inlet/outlet
  • One 1/4" compression tube fitting each side as gas inlet and outlet
  • One 1/4" quick-connect port for in-situ temperature measurement
  • One KF25 port for vacuum generation
Pressure Gauge
  • Inficon PCG 554 ceramic coated Pirani capacitance diaphragm pressure gauge, 3.8e-5 … 1125 torr
Gas Flow
  • 1-1000 sccm mass flow controller
Sample Stage
   
  • A quartz sample stage with 8 cavities.
  • 8 quartz crucibles Ø21 × 25 mm (6 mL)
  • Crucibles in different materials, such as alumina, graphite, magnesia, are available upon request.
  • Wafer holders for 1-4" are also available upon request. 
  • Customized sample holder/crucible is also available upon request
Thermal Block
Control Panel & Software

  • LabVIEW based software for remote PC control, monitoring, and data logging 
  • Complimentary Python API
  • Ethernet TCP/IP communication port
  • PC operation software supports 8 sets of furnaces
  • One laptop with preinstalled software and communication cables. 
Robotic Arm (Optional)
Desktop Collaborative Robot - MTI-MG400

  • Automated sample loading and retrieval via an integrated robotic arm. 
  • Power: 48VDC, 150W
  • Maximum load: 5kg
  • Accuracy: ±0.02 mm
Vacuum Pump
  • 240L/min rotary vane pump is included. 
  • Pump is connected with and controlled by the furnace.
Chilled Water
Application Notes

  • The furnace can be integrated with dosing, mixing, milling, and pellet pressing equipment to achieve an automated high temperature materials synthesis platform. 
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Compliance
  • NRTL or CSA certification is available upon request at an extra cost.